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more work moving stuff from wiki into github doc
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bruceravel committed Jan 30, 2024
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2 changes: 1 addition & 1 deletion devtools/conda-envs/docs_env.yaml
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Expand Up @@ -20,5 +20,5 @@ dependencies:
- sphinx-math-dollar
- sphinx-subfigure
- sphinx-design

- sphinxcontrib.bibtex

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2 changes: 2 additions & 0 deletions docs/automation.rst
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Expand Up @@ -189,6 +189,8 @@ was called :file:`mysamples`, the new BlueSky command is called
Convert spreadsheets to Bluesky queueserver input.


.. _sample_wheel_automation:

Sample wheel automation
-----------------------

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200 changes: 200 additions & 0 deletions docs/before.rst
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..
This document was developed primarily by a NIST employee. Pursuant
to title 17 United States Code Section 105, works of NIST employees
are not subject to copyright protection in the United States. Thus
this repository may not be licensed under the same terms as Bluesky
itself.
See the LICENSE file for details.

.. _before:

Before your Beamtime
====================

Register for BNL Site Access
----------------------------

Upon receipt of notification of your beamtime, verify that all
the team members attending your experiment have a valid BNL Guest
registration.

.. note::

+ New registration requests as well as the extensions requests for
expired registrations shall be submitted as soon as possible.
+ Approvals for guest registrations can take as long as two
months for some non-US citizens.

To apply for a BNL Guest appointment: https://www.bnl.gov/ps/userguide/beforearrival.php

.. caution:: Without an active appointment, you will not be allowed
on site and will be turned away at the main gate.

BNL Domain Account
------------------

When your BNL Guest registration becomes active, you should receive an
email with instructions for enabling your BNL domain account. You must
complete that step, which includes setting your password and signing
up for DUO Federal two-factor authentication. If you need to request
an account, go to https://www.bnl.gov/accounts/ and click the button
that says "Submit account registration form".

Enabling your BNL account is non-optional. You must have an active
account in order to unlock the computers at the beamline.

.. caution:: Without an active account, a known password, and DUO
Federal two-factor authentication, you will be unable to
perform your experiment.

Safety Approval Form
--------------------

Submit your Safety Approval Form (SAF) AT LEAST two weeks before the
above starting date. Your SAF should provide a complete and accurate
description of the experiment, including all samples, chemicals,
solvents, reference materials, and equipment that will be used during
the experiment and preparation. In addition, any additional equipment
not provided by the beamline has to be identified and described in the
SAF. Provide detailed information on sample processing and any safety
measures necessary.

.. caution:: An approved SAF is required on the first day of beamtime.
Without enough time for approval, you may lose your
beamtime beamtime.

To submit a SAF: https://pass.bnl.gov

If your experiment requires chemicals, compressed gases, lab access,
or other equipment, please contact `Bruce Ravel
<mailto:[email protected]>`__ well ahead of your expriment.
Transportation of hazardous materials related to your experiment to
the BNL site and back to the home institution is your responsibility.


Support Laboratories
--------------------

Currently, four labs support user activities at BMM. They are:

+ Lab 3L-L06: XAS Sample Prep Lab
+ Lab 3L-L07: Environmental Science Wet Lab
+ Lab 3L-L09: XAS Chemistry Lab
+ Lab 4L-L09: Electrochemistry Lab

See https://www.bnl.gov/nsls2/labs/

If you prepare or treat samples on-site, you must request use of the
appropriate NSLS-II User Laboratory when you submit your Safety
Approval Form.

You cannot request a laboratory after an SAF has been approved.


Here is some advice on selecting the correct lab:

Unbound nanoparticles
Please note that supported nanoparticles or nanoparticles in
solution are not considered “unbound”. If your samples are indeed
unbound, please contact BMM beamline scientist Bruce Ravel
([email protected]) as soon as possible.

Solid sample preparation (pellet pressing, spreading on tape etc)
Request Lab 3L-L06.

Liquid samples (organic solvents, acids, bases)
Request Lab 3L-L09.

Hydrofluoric acid treatment
Request Lab 3L-L09 and notify Cognizant Space Manager, Syed Khalid
at [email protected], as soon as possible.

Environment and earth science sample preparation and treatment
Request Lab 3L-L07.

Electrochemistry and battery science
Request Lab 4L-L09.

Radionuclide samples must be prepared and properly contained at the
home institution. NSLS-II has no lab available for work on
radiological materials. Samples with depleted uranium and uranium at
low or environmentally relevant concentrations are considered
radiological samples at NSLS-II and must be treated accordingly.

Requests for using gloveboxes should be discussed prior to submitting
the SAF, with Bruce Ravel ([email protected]) and/or Syed Khalid
([email protected])

.. note:: Each lab you select on your safety approval form makes work
for the lab stewards. Only request the lab(s) that you
actually intend to use.

Training
--------

Please complete all required online user training at least one week
before the starting date. Failure to complete training will result in a
delay starting your experiment.

To complete your training, follow the training instructions at:
https://www.bnl.gov/ps/userguide/beforearrival.php


Electrical Equipment
--------------------

Any equipment with an electrical cable including low-voltage
instruments and sample holderss are considered electrical equipment
(laptop computers are excluded).

If you plan to bring electrical equipment for your experiment, please
contact Jerome Malley, Electrical Equipment Inspection (EEI) Manager
at [email protected] as soon as practical and at least two weeks before
the start of your experiment. Be prepared to provide manuals, photos,
electrical diagrams, and schematics.

Please include beamline staff (Bruce Ravel <[email protected]> for all
experiments; Vesna Stanic <[email protected]> & Jean Jordan-Sweet
<[email protected]> for XRD experiments) in your communication as some
pre-approved electrical equipment (e.g., potentiostat, heaters,
temperature meters, and controllers) may be available at the beamline.

.. note:: Failure to comply with EEI will result in a delay to your
experiment. Equipment that cannot pass EEI may not be used
at NSLS-II.

Research Equipment Pool
-----------------------

Many experimental tools are available from `the NSLS-II Research
Equipment Pool
<https://public.bnl.gov/sites/rep/SitePages/Home.aspx>`__. If you
wish to use any items from equipment pool, contact `Bruce Ravel
<mailto:[email protected]>`__ well ahead of your experiment.


Shipping things to the beamline
-------------------------------

Things should be shipped to

.. code-block:: none
Bruce Ravel / Beamline 6BM
Building 740
Brookhaven National Laboratory
Upton NY 11973
The Day of your Experiment
--------------------------

.. note:: Unless told otherwise, your experiment starts at 8 am.

You should consider having all team members arrive the afternoon prior
to the first day of the beamtime to check in at `the GUV Center
<https://www.bnl.gov/guv/>`__ and to complete beamline specific
training.

Please consult `NSLS-II user guide <https://www.bnl.gov/ps/userguide/>`__
or contact BMM beamline staff for more information.
55 changes: 55 additions & 0 deletions docs/commonchores.rst
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Expand Up @@ -15,6 +15,61 @@
Common chores
=============

Search the Hutch
----------------

The buttons on the hutch interlock panel are labeled with black
stickers with white numbers. Those labels correspond to the numbering
in these lists:

To OPEN the hutch
~~~~~~~~~~~~~~~~~

+ 6. Close the shutter
+ 5. Press the "SBE" button
+ 4. ∙∙∙
+ 3. Make sure the “Front Left Maglock” button is not green
+ 2. Press the green “Open Door” button, wait for the slow door to open
+ 1. Enter the hutch


To CLOSE the hutch
~~~~~~~~~~~~~~~~~~

Everyone but the person performing the search should leave the hutch.

The search is done by and only one person. Only one person pushes all
the buttons. The serach **is not** a team sport!

1. Complete the hutch search

+ Look in the mirror to see that no one is behind the table
+ Press search button 1
+ Visually inspect the length of the hutch, verifying that it is empty of people
+ Press search button 2
+ Exit the hutch

2. ∙∙∙
3. Push the “Front Left Maglock” button. It should be lit green
4. Push and hold the yellow “Close Door” button. Listen for the magnetic latch
5. Push the "SBE" button, wait for the loud noise to finish
6. You can now open the shutter

Hutch search sign
~~~~~~~~~~~~~~~~~

These instructions are printed, laminated, mounted on a magnetic
sheet, and hung near the search station. I would like to make these
signs in various languages. If you would like to help by translating
this sign, download the Word document below. Make a translation into
your language and mail the Word doc back to Bruce. He will print and
mount the new translation! I am most eager for Chinese, Russian, and
German translations.

:download:`Word document with hutch search instructions <_static/HutchSearch.docx>`.



Change energy and prepare for fluorescence measurements
-------------------------------------------------------

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4 changes: 2 additions & 2 deletions docs/details.rst
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Expand Up @@ -114,8 +114,8 @@ Bluesky. The heart of the implementation is a system call to
``fswebcam``. From there, the image is saved as an asset and correctly
pointed to in databroker. See:

+ https://github.com/NSLS-II-BMM/profile_collection/blob/master/startup/BMM/user_ns/detectors.py#L253
+ https://github.com/NSLS-II-BMM/profile_collection/blob/master/startup/BMM/camera_device.py#L62-L164
+ `BMM/user_ns/detectors.py <https://github.com/NSLS-II-BMM/profile_collection/blob/master/startup/BMM/user_ns/detectors.py#L253>`__
+ `BMM/camera_device.py <https://github.com/NSLS-II-BMM/profile_collection/blob/master/startup/BMM/camera_device.py#L62-L164>`__


DI Water Flow
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3 changes: 2 additions & 1 deletion docs/index.rst
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Expand Up @@ -21,6 +21,7 @@ BMM is NIST's Beamline for Materials Measurement
:caption: Running the beamline

intro.rst
before.rst
instruments.rst
motors.rst
pds.rst
Expand All @@ -29,8 +30,8 @@ BMM is NIST's Beamline for Materials Measurement
automation.rst
log.rst
manage.rst
cheatsheet.rst
commonchores.rst
cheatsheet.rst
trouble.rst

.. appendix::
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