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more work moving stuff from wiki into github doc
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.. | ||
This document was developed primarily by a NIST employee. Pursuant | ||
to title 17 United States Code Section 105, works of NIST employees | ||
are not subject to copyright protection in the United States. Thus | ||
this repository may not be licensed under the same terms as Bluesky | ||
itself. | ||
See the LICENSE file for details. | ||
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||
.. _before: | ||
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Before your Beamtime | ||
==================== | ||
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Register for BNL Site Access | ||
---------------------------- | ||
|
||
Upon receipt of notification of your beamtime, verify that all | ||
the team members attending your experiment have a valid BNL Guest | ||
registration. | ||
|
||
.. note:: | ||
|
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+ New registration requests as well as the extensions requests for | ||
expired registrations shall be submitted as soon as possible. | ||
+ Approvals for guest registrations can take as long as two | ||
months for some non-US citizens. | ||
|
||
To apply for a BNL Guest appointment: https://www.bnl.gov/ps/userguide/beforearrival.php | ||
|
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.. caution:: Without an active appointment, you will not be allowed | ||
on site and will be turned away at the main gate. | ||
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BNL Domain Account | ||
------------------ | ||
|
||
When your BNL Guest registration becomes active, you should receive an | ||
email with instructions for enabling your BNL domain account. You must | ||
complete that step, which includes setting your password and signing | ||
up for DUO Federal two-factor authentication. If you need to request | ||
an account, go to https://www.bnl.gov/accounts/ and click the button | ||
that says "Submit account registration form". | ||
|
||
Enabling your BNL account is non-optional. You must have an active | ||
account in order to unlock the computers at the beamline. | ||
|
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.. caution:: Without an active account, a known password, and DUO | ||
Federal two-factor authentication, you will be unable to | ||
perform your experiment. | ||
|
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Safety Approval Form | ||
-------------------- | ||
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Submit your Safety Approval Form (SAF) AT LEAST two weeks before the | ||
above starting date. Your SAF should provide a complete and accurate | ||
description of the experiment, including all samples, chemicals, | ||
solvents, reference materials, and equipment that will be used during | ||
the experiment and preparation. In addition, any additional equipment | ||
not provided by the beamline has to be identified and described in the | ||
SAF. Provide detailed information on sample processing and any safety | ||
measures necessary. | ||
|
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.. caution:: An approved SAF is required on the first day of beamtime. | ||
Without enough time for approval, you may lose your | ||
beamtime beamtime. | ||
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To submit a SAF: https://pass.bnl.gov | ||
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If your experiment requires chemicals, compressed gases, lab access, | ||
or other equipment, please contact `Bruce Ravel | ||
<mailto:[email protected]>`__ well ahead of your expriment. | ||
Transportation of hazardous materials related to your experiment to | ||
the BNL site and back to the home institution is your responsibility. | ||
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Support Laboratories | ||
-------------------- | ||
|
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Currently, four labs support user activities at BMM. They are: | ||
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+ Lab 3L-L06: XAS Sample Prep Lab | ||
+ Lab 3L-L07: Environmental Science Wet Lab | ||
+ Lab 3L-L09: XAS Chemistry Lab | ||
+ Lab 4L-L09: Electrochemistry Lab | ||
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See https://www.bnl.gov/nsls2/labs/ | ||
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If you prepare or treat samples on-site, you must request use of the | ||
appropriate NSLS-II User Laboratory when you submit your Safety | ||
Approval Form. | ||
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You cannot request a laboratory after an SAF has been approved. | ||
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Here is some advice on selecting the correct lab: | ||
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Unbound nanoparticles | ||
Please note that supported nanoparticles or nanoparticles in | ||
solution are not considered “unbound”. If your samples are indeed | ||
unbound, please contact BMM beamline scientist Bruce Ravel | ||
([email protected]) as soon as possible. | ||
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Solid sample preparation (pellet pressing, spreading on tape etc) | ||
Request Lab 3L-L06. | ||
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Liquid samples (organic solvents, acids, bases) | ||
Request Lab 3L-L09. | ||
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Hydrofluoric acid treatment | ||
Request Lab 3L-L09 and notify Cognizant Space Manager, Syed Khalid | ||
at [email protected], as soon as possible. | ||
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Environment and earth science sample preparation and treatment | ||
Request Lab 3L-L07. | ||
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Electrochemistry and battery science | ||
Request Lab 4L-L09. | ||
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Radionuclide samples must be prepared and properly contained at the | ||
home institution. NSLS-II has no lab available for work on | ||
radiological materials. Samples with depleted uranium and uranium at | ||
low or environmentally relevant concentrations are considered | ||
radiological samples at NSLS-II and must be treated accordingly. | ||
|
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Requests for using gloveboxes should be discussed prior to submitting | ||
the SAF, with Bruce Ravel ([email protected]) and/or Syed Khalid | ||
([email protected]) | ||
|
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.. note:: Each lab you select on your safety approval form makes work | ||
for the lab stewards. Only request the lab(s) that you | ||
actually intend to use. | ||
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Training | ||
-------- | ||
|
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Please complete all required online user training at least one week | ||
before the starting date. Failure to complete training will result in a | ||
delay starting your experiment. | ||
|
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To complete your training, follow the training instructions at: | ||
https://www.bnl.gov/ps/userguide/beforearrival.php | ||
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Electrical Equipment | ||
-------------------- | ||
|
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Any equipment with an electrical cable including low-voltage | ||
instruments and sample holderss are considered electrical equipment | ||
(laptop computers are excluded). | ||
|
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If you plan to bring electrical equipment for your experiment, please | ||
contact Jerome Malley, Electrical Equipment Inspection (EEI) Manager | ||
at [email protected] as soon as practical and at least two weeks before | ||
the start of your experiment. Be prepared to provide manuals, photos, | ||
electrical diagrams, and schematics. | ||
|
||
Please include beamline staff (Bruce Ravel <[email protected]> for all | ||
experiments; Vesna Stanic <[email protected]> & Jean Jordan-Sweet | ||
<[email protected]> for XRD experiments) in your communication as some | ||
pre-approved electrical equipment (e.g., potentiostat, heaters, | ||
temperature meters, and controllers) may be available at the beamline. | ||
|
||
.. note:: Failure to comply with EEI will result in a delay to your | ||
experiment. Equipment that cannot pass EEI may not be used | ||
at NSLS-II. | ||
|
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Research Equipment Pool | ||
----------------------- | ||
|
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Many experimental tools are available from `the NSLS-II Research | ||
Equipment Pool | ||
<https://public.bnl.gov/sites/rep/SitePages/Home.aspx>`__. If you | ||
wish to use any items from equipment pool, contact `Bruce Ravel | ||
<mailto:[email protected]>`__ well ahead of your experiment. | ||
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Shipping things to the beamline | ||
------------------------------- | ||
|
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Things should be shipped to | ||
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.. code-block:: none | ||
Bruce Ravel / Beamline 6BM | ||
Building 740 | ||
Brookhaven National Laboratory | ||
Upton NY 11973 | ||
The Day of your Experiment | ||
-------------------------- | ||
|
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.. note:: Unless told otherwise, your experiment starts at 8 am. | ||
|
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You should consider having all team members arrive the afternoon prior | ||
to the first day of the beamtime to check in at `the GUV Center | ||
<https://www.bnl.gov/guv/>`__ and to complete beamline specific | ||
training. | ||
|
||
Please consult `NSLS-II user guide <https://www.bnl.gov/ps/userguide/>`__ | ||
or contact BMM beamline staff for more information. |
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