From 745398edc069fe01257e03daa10ea32cbb5fd220 Mon Sep 17 00:00:00 2001 From: Nicole Jung Date: Fri, 19 Jul 2024 22:47:43 +0200 Subject: [PATCH] Update HPLC.mdx --- docs/repo/details_standards/analysis_test/HPLC.mdx | 5 +++-- 1 file changed, 3 insertions(+), 2 deletions(-) diff --git a/docs/repo/details_standards/analysis_test/HPLC.mdx b/docs/repo/details_standards/analysis_test/HPLC.mdx index 41a4ce00..02e18049 100644 --- a/docs/repo/details_standards/analysis_test/HPLC.mdx +++ b/docs/repo/details_standards/analysis_test/HPLC.mdx @@ -14,10 +14,11 @@ Updated: 19.07.2024 ## Inline notation for HPLC data -The inline notation gives a short summary of the metadata and a list of all sials or signals group (for signals that cannot be separated from each other). For each signal, the shift should be provided along with at least the following information given in parentheses: multiplet abbreviations, coupling constants, and number of atoms represented by each signal should be provided. (see **example No 1**) +The inline notation gives a short summary of the metadata and a list of all peaks/curves. For each peak, the retention time (ret) should be provided in minutes along with the area under the curve given in %. In squared brackets, the assignment to a molecule (if known) can be given. The total area under the curve should be 100% - if not all curves can be defined, the rest % can be given as "others (xx%)". After the listing of single peaks/curves, the final evaluation of the measurement can be given, e.g. 57% conversion. +(see **example No 1**) ### Examples for desired formatting: **(1) Standard example:** -HPLC (VDSpher 100, C18-E, 5 μm, 250 x 4.0 mm; 20 °C; ACN/H2O 10:90 (0-1 min), 10:90 to 99:1 (1-11 min), 99:1 (11-14 min), 99:1 to 10:90 (14-16 min), 10:90 (16-20 min), 1 mL/min; 230 nm): ret [min] (area [%]) = 10.720 (36) [triazine], 7.802 (47) [indazole], others (17%). Conversion of indazole: 57% +HPLC (VDSpher 100, C18-E, 5 μm, 250 x 4.0 mm; 20 °C; ACN/H2O 10:90 (0-1 min), 10:90 to 99:1 (1-11 min), 99:1 (11-14 min), 99:1 to 10:90 (14-16 min), 10:90 (16-20 min), 1 mL/min; 230 nm): ret [min] (area [%]) = 10.720 (36) [triazine], 7.802 (47) [indazole], others (17%). Conversion of indazole: 57%.